{"id":62866,"date":"2024-05-10T14:04:15","date_gmt":"2024-05-10T18:04:15","guid":{"rendered":"https:\/\/www.crchudequebec.ulaval.ca\/analyse-structurale-moleculaire\/"},"modified":"2024-07-09T10:05:20","modified_gmt":"2024-07-09T14:05:20","slug":"structural-molecular-analysis","status":"publish","type":"page","link":"https:\/\/www.crchudequebec.ulaval.ca\/en\/platforms-and-services\/medicinal-chemistry\/structural-molecular-analysis\/","title":{"rendered":"Structural Molecular Analysis"},"content":{"rendered":"<section class=\"bg-white align wp-block-acf-content-with-left-sidebar\">\n    <div class=\"container\">\n    <div class=\"padd padd--bottom\">\n        <div class=\"wrap\">\n            <div class=\"flex md:flex-row flex-col md:gap-x-[8.3%] gap-x-3 md:gap-y-0 gap-y-8\">\n                <div class=\"sidebar md:w-1\/4 w-full flex flex-col gap-y-8\">\n                    \n                    \n                                                                        <div>\n                                                                    <h3 class=\"mb-0 text-16 font-bold\">Director<\/h3>\n                                \n                                                                    <div class=\"mb-1\">\n                                        Donald Poirier, Ph.D.\n                                    <\/div>\n                                \n                                                                    <div class=\"mb-1\">\n                                                                                    \n                                            <a class=\"phone\" href=\"tel:418-654-2296\u202f; 418-525-4444 (ext 46427)  \">418-654-2296\u202f; 418-525-4444 (ext 46427)  <\/a>\n                                                                            <\/div>\n                                \n                                                                    <ul class=\"emails !mb-3\">\n                                                                                    <li class=\"overflow-hidden\">\n                                                <a class=\"group flex items-center\" href=\"mailto:Donald.poirier@crchudequebec.ulaval.ca\" title=\"Donald.poirier@crchudequebec.ulaval.ca\">\n                                                    <i class=\"fa-light fa-envelope shrink-0 group-hover:text-blue-500 duration-300\"><\/i>\n                                                    <span class=\"text-16 whitespace-nowrap overflow-hidden text-ellipsis group-hover:text-blue-500 duration-300\">Donald.poirier@crchudequebec.ulaval.ca<\/span>\n                                                <\/a>\n                                            <\/li>\n                                                                            <\/ul>\n                                \n                                                            <\/div>\n                                                    <div>\n                                                                    <h3 class=\"mb-0 text-16 font-bold\">Manager<\/h3>\n                                \n                                                                    <div class=\"mb-1\">\n                                        Ren\u00e9 Maltais, Ph.D.\n                                    <\/div>\n                                \n                                                                    <div class=\"mb-1\">\n                                                                                    \n                                            <a class=\"phone\" href=\"tel:418-654-2296, 418-525-4444 (ext 46428)\">418-654-2296, 418-525-4444 (ext 46428)<\/a>\n                                                                            <\/div>\n                                \n                                                                    <ul class=\"emails !mb-3\">\n                                                                                    <li class=\"overflow-hidden\">\n                                                <a class=\"group flex items-center\" href=\"mailto:Rene.maltais@crchudequebec.ulaval.ca\" title=\"Rene.maltais@crchudequebec.ulaval.ca\">\n                                                    <i class=\"fa-light fa-envelope shrink-0 group-hover:text-blue-500 duration-300\"><\/i>\n                                                    <span class=\"text-16 whitespace-nowrap overflow-hidden text-ellipsis group-hover:text-blue-500 duration-300\">Rene.maltais@crchudequebec.ulaval.ca<\/span>\n                                                <\/a>\n                                            <\/li>\n                                                                            <\/ul>\n                                \n                                                            <\/div>\n                                                    <div>\n                                                                    <h3 class=\"mb-0 text-16 font-bold\">Project Leader<\/h3>\n                                \n                                                                    <div class=\"mb-1\">\n                                        Jean-Yves Sanc\u00e9au, Ph.D. \n                                    <\/div>\n                                \n                                                                    <div class=\"mb-1\">\n                                                                                    \n                                            <a class=\"phone\" href=\"tel:418-654-2296\">418-654-2296<\/a>\n                                                                            <\/div>\n                                \n                                                                    <ul class=\"emails !mb-3\">\n                                                                                    <li class=\"overflow-hidden\">\n                                                <a class=\"group flex items-center\" href=\"mailto:Jean-yves.sanceau@crchudequebec.ulaval.ca\" title=\"Jean-yves.sanceau@crchudequebec.ulaval.ca\">\n                                                    <i class=\"fa-light fa-envelope shrink-0 group-hover:text-blue-500 duration-300\"><\/i>\n                                                    <span class=\"text-16 whitespace-nowrap overflow-hidden text-ellipsis group-hover:text-blue-500 duration-300\">Jean-yves.sanceau@crchudequebec.ulaval.ca<\/span>\n                                                <\/a>\n                                            <\/li>\n                                                                            <\/ul>\n                                \n                                                            <\/div>\n                                            \n                    \n                    \n                    \n                                    <\/div>\n                <div class=\"main-content md:w-7\/12 w-full\">\n                                            <figure class=\"md:mb-12 mb-6\">\n                            <img loading=\"lazy\" decoding=\"async\" width=\"1920\" height=\"1080\" src=\"https:\/\/www.crchudequebec.ulaval.ca\/wp-content\/uploads\/2024\/04\/Plateforme_chimiemedicinale_Analysemoleculaire-1920x1080.jpg\" class=\"rounded-3xl\" alt=\"\" \/>\n\n                                                    <\/figure>\n                    \n                    \n                                            <div class=\"content\">\n                            <div class=\"inner\">\n                                <p><span data-contrast=\"none\">We can assist you in the structural analysis of your molecules of interest using different cutting-edge technologies such as nuclear magnetic resonance (NMR), mass spectrometry (LRMS), infrared analysis (FTIR) and purity analysis (HPLC). We have a Bruker Ascend-300 MHz NMR device. We can record spectra to assist you in determining an unknown molecular structure or in the more complete characterization of a molecule.<\/span><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335551550&quot;:6,&quot;335551620&quot;:6,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<p><b><span data-contrast=\"auto\">Nuclear Magnetic Resonance (NMR) Spectrum<\/span><\/b><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335551550&quot;:6,&quot;335551620&quot;:6,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<p><span data-contrast=\"auto\">The laboratory has a Bruker 300 MHz NMR which allows different experiments such as:<\/span><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335551550&quot;:6,&quot;335551620&quot;:6,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<ul>\n<li><span data-contrast=\"auto\"> Routine <\/span><sup><span data-contrast=\"auto\">1<\/span><\/sup><span data-contrast=\"auto\">H NMR and <\/span><sup><span data-contrast=\"auto\">13<\/span><\/sup><span data-contrast=\"auto\">C NMR (APT)<\/span><\/li>\n<li><span data-contrast=\"auto\"> 2D experience (NOESY, COZY, HSQC, HMBC, ROESY, TOCSY)<\/span><\/li>\n<li><span data-contrast=\"auto\"> NMR of heteroatoms: <\/span><sup><span data-contrast=\"auto\">11<\/span><\/sup><span data-contrast=\"auto\">B, <\/span><sup><span data-contrast=\"auto\">31<\/span><\/sup><span data-contrast=\"auto\">P, <\/span><sup><span data-contrast=\"auto\">19<\/span><\/sup><span data-contrast=\"auto\">F, Other nuclei on request<\/span><\/li>\n<li><span data-contrast=\"auto\"> High temperature experiments<\/span><\/li>\n<\/ul>\n<p><b><span data-contrast=\"auto\">Mass Spectrum (LRMS)<\/span><\/b><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335551550&quot;:6,&quot;335551620&quot;:6,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<p><span data-contrast=\"auto\">The laboratory has a LCMS-2020 mass spectrometer from Shimadzu. The device is equipped with DUIS and APCI probes allowing the ionization of a wide variety of products. In addition to assisting medicinal chemistry laboratory professionals in their research, we can offer a mass determination service.<\/span><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335551550&quot;:6,&quot;335551620&quot;:6,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<p><b><span data-contrast=\"auto\">HPLC purity<\/span><\/b><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335551550&quot;:6,&quot;335551620&quot;:6,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<p><span data-contrast=\"auto\">The laboratory has a Prominence liquid chromatography device from Shimadzu with UV detector. The system is coupled to an LCMS-2020 mass spectrometer. It is therefore possible for us to offer purity analyzes either by UV detection or by mass detection. This service, adapted to the specific needs of applicants, is offered to researchers at the CRCHU de Qu\u00e9bec as well as to external researchers.\u00a0<\/span><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335551550&quot;:6,&quot;335551620&quot;:6,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<h4><strong>Pricing<\/strong><\/h4>\n<p><b><span data-contrast=\"auto\">Nuclear magnetic resonance (NMR) spectrum<\/span><\/b><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<ul>\n<li><span data-contrast=\"auto\">H NMR: $35\/sample; APT $70\/hour (maximum of 3 hours billed);<\/span><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335559740&quot;:259}\">\u00a0<\/span><\/li>\n<li><span data-contrast=\"auto\">D experience: $80 maximum of 3 hours billed per sample for acquisition and $70\/hour for processing.*<\/span><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335559740&quot;:259}\">\u00a0<\/span><\/li>\n<\/ul>\n<p><b><span data-contrast=\"auto\">Mass Spectrum (LRMS)<\/span><\/b><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<ul>\n<li><span data-contrast=\"auto\">Mass analyses: $35; price for more than 10 samples $20*<\/span><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335559740&quot;:259}\">\u00a0<\/span><\/li>\n<\/ul>\n<p><b><span data-contrast=\"auto\">HPLC purity<\/span><\/b><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335559740&quot;:259}\">\u00a0<\/span><\/p>\n<ul>\n<li><span data-contrast=\"auto\">HPLC-MS purity analyses: $100; price for more than 10 samples $50*<\/span><span data-ccp-props=\"{&quot;201341983&quot;:0,&quot;335559740&quot;:259}\">\u00a0<\/span><\/li>\n<\/ul>\n<p>*Researchers from CHU de Qu\u00e9bec-Universit\u00e9 Laval will benefit from a 20% discount on displayed rates.<\/p>\n\n                            <\/div>\n                        <\/div>\n                    \n                    \n                    \n                    \n                                    <\/div>\n            <\/div>\n        <\/div>\n    <\/div>\n<\/div>\n<\/section>\n\n\n<section id=\"\" data-block=\"block_5eaedcdc48e2bdb242a1b5f92adabfbf\" class=\"block-useful-links align bg-white\">\n        <div class=\"container\">\n            <div class=\"padd\">\n                <div class=\"wrap\">\n                                            <h2 class=\"sm:text-48 text-36 !font-bold !leading-tight !mb-10 lg:!mb-16\">Equipment<\/h2>\n                    \n                                                                        <a\n                                href=\"https:\/\/www.bruker.com\/en\/products-and-solutions\/mr\/nmr\/ascend-nmr-magnets.html\"\n                                title=\"NMR (300 MHz) Bruker\"\n                                target=\"_blank\"\n                                class=\"block relative w-full py-5 md:py-8 pl-4 md:pl-10 pr-24 border-t border-blue-200 last:border-b font-semibold text-16 sm:text-20 lg:text-24 bg-white hover:bg-blue-100 duration-500\"\n                            >\n                                <span>NMR (300 MHz) Bruker<\/span>\n                                <i class=\"absolute top-1\/2 -translate-y-1\/2 right-4 md:right-10 fa-light fa-arrow-up-right text-20 sm:text-24 lg:text-30\"><\/i>\n                            <\/a>\n                                                                                                <a\n                                href=\"https:\/\/www.shimadzu.com\/an\/case-studies\/high-performance-liq\/index.html\"\n                                title=\"LC-MS (semi-preparative) Shimadzu\"\n                                target=\"_blank\"\n                                class=\"block relative w-full py-5 md:py-8 pl-4 md:pl-10 pr-24 border-t border-blue-200 last:border-b font-semibold text-16 sm:text-20 lg:text-24 bg-white hover:bg-blue-100 duration-500\"\n                            >\n                                <span>LC-MS (semi-preparative) Shimadzu<\/span>\n                                <i class=\"absolute top-1\/2 -translate-y-1\/2 right-4 md:right-10 fa-light fa-arrow-up-right text-20 sm:text-24 lg:text-30\"><\/i>\n                            <\/a>\n                                                                                                <a\n                                href=\"https:\/\/new.abb.com\/products\/measurement-products\/analytical\/ft-ir-and-ft-nir-analyzers\"\n                                title=\"Fourier transform infrared (FTIR) ABB system\"\n                                target=\"_blank\"\n                                class=\"block relative w-full py-5 md:py-8 pl-4 md:pl-10 pr-24 border-t border-blue-200 last:border-b font-semibold text-16 sm:text-20 lg:text-24 bg-white hover:bg-blue-100 duration-500\"\n                            >\n                                <span>Fourier transform infrared (FTIR) ABB system<\/span>\n                                <i class=\"absolute top-1\/2 -translate-y-1\/2 right-4 md:right-10 fa-light fa-arrow-up-right text-20 sm:text-24 lg:text-30\"><\/i>\n                            <\/a>\n                                                            <\/div>\n            <\/div>\n        <\/div>\n    <\/section>\n","protected":false},"excerpt":{"rendered":"<p>We can assist you in the structural analysis of your molecules of interest using different cutting-edge technologies (NMR, LC-MS, FTIR, etc.)<\/p>\n","protected":false},"author":37,"featured_media":0,"parent":62904,"menu_order":1,"comment_status":"closed","ping_status":"closed","template":"template-platforms-services.blade.php","meta":{"_acf_changed":false,"inline_featured_image":false,"footnotes":"","_links_to":"","_links_to_target":""},"class_list":["post-62866","page","type-page","status-publish","hentry"],"acf":[],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v25.5 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ 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